HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium cyanoborohydride → 6,7-dichloro-2,3-dihydro-1H-indole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium cyanoborohydride | HCID 5003444 | — |
| Reactant | 6,7-dichloro-1H-indole | HCID 12272802 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | 6,7-dichloro-2,3-dihydro-1H-indole | HCID 16788296 | 67% |
Reaction Steps
6,7-Dichloroindole (D33) was reduced in the usual way with sodium cyanoborohydride in glacial acetic acid to give the title compound (D34) (1.14 g, 67%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05834494 |
| Source dataset | uspto-grants-1998_11 |
| ORD ID | ord-d878c630a6364c65836ead566b44736b |
| Source note | uspto-grants-1998_11 |