HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium cyanoborohydride → 6-Chloro-5-methylthioindoline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium cyanoborohydride | HCID 5003444 | — |
| Reactant | 6-Chloro-5-methylthioindole | HCID 10559858 | — |
| Product | 6-Chloro-5-methylthioindoline | HCID 10559934 | 98.8% |
Reaction Steps
6-Chloro-5-methylthioindole (D47) (0.72 g, 3.65 mmol) was treated with sodium cyanoborohydride as in the method of Description 10 to give the title compound (0.72 g, 98%) as a pale yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05834494 |
| Source dataset | uspto-grants-1998_11 |
| ORD ID | ord-c3f24d915a3d42d1b09b54ad2d686ba6 |
| Source note | uspto-grants-1998_11 |