HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium cyanoborohydride → 6-Chloro-5-ethylthioindoline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium cyanoborohydride | HCID 5003444 | — |
| Reactant | 6-Chloro-5-ethylthioindole | HCID 18940927 | — |
| Product | 6-Chloro-5-ethylthioindoline | HCID 18940911 | 57% |
Reaction Steps
6-Chloro-5-ethylthioindole (D63) (0.35 g, 1.67 mmol) was treated with sodium cyanoborohydride as in the method of Description 10 to give the title compound (0.18 g, 57%) as a yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05834494 |
| Source dataset | uspto-grants-1998_11 |
| ORD ID | ord-dd0ee8a0265847ea8360e87fcccd60e9 |
| Source note | uspto-grants-1998_11 |