3-Isocyanatopyridine → HCID 10566712, compound

HRID 356049Notes

Reaction equation

HRID 356049 reaction equation
[N:1]1[CH:6]=[CH:5][CH:4]=[C:3]([N:7]=[C:8]=[O:9])[CH:2]=1.[Cl:10][C:11]1[C:19]([Cl:20])=[CH:18][CH:17]=[C:16]2[C:12]=1[CH2:13][CH2:14][NH:15]2>>[Cl:10][C:11]1[C:19]([Cl:20])=[CH:18][CH:17]=[C:16]2[C:12]=1[CH2:13][CH2:14][N:15]2[C:8](=[O:9])[NH:7][C:3]1[CH:2]=[N:1][CH:6]=[CH:5][CH:4]=1

Participants

3

Procedure

The title compound was prepared as in the method of (Example 2) from 3-pyridylisocyanate and 4,5-dichloroindoline (D32) to give (E16) (0.5 g, 25%) m.p. >240° C.

Workup

  1. customto give (E16) (0.5 g, 25%) m.p. >240° C.

Sources & evidence

ORD record
ord-54f664aa75a445329900b154afc84d0b
Source dataset
uspto-grants-1998_11
Patent number
US05834494

Reaction notes

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