5-Chloroindoline → HCID 10826147, compound

HRID 356051Notes

Reaction equation

HRID 356051 reaction equation
[N:1]1[CH:6]=[CH:5][CH:4]=[C:3]([N:7]=[C:8]=[O:9])[CH:2]=1.[Cl:10][C:11]1[CH:12]=[C:13]2[C:17](=[CH:18][CH:19]=1)[NH:16][CH2:15][CH2:14]2>>[Cl:10][C:11]1[CH:12]=[C:13]2[C:17](=[CH:18][CH:19]=1)[N:16]([C:8](=[O:9])[NH:7][C:3]1[CH:2]=[N:1][CH:6]=[CH:5][CH:4]=1)[CH2:15][CH2:14]2

Participants

3

Reactant 2

HCID 1175965-ChloroindolineHCID 27604933-Isocyanatopyridine

Product 1

HCID 10826147HCID 10826147, compound

Procedure

The title compound was prepared as in the method of (Example 2) from 3-pyridylisocyanate and 5-chloroindoline (D35) to give (E18) (1.4 g, 82%) m.p. 204°-5° C.

Workup

  1. customto give (E18) (1.4 g, 82%) m.p. 204°-5° C.

Sources & evidence

ORD record
ord-dedceafe4ab64b609a5106c896817f12
Source dataset
uspto-grants-1998_11
Patent number
US05834494

Reaction notes

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