3-Isocyanatopyridine → HCID 10590892, compound

HRID 356053Notes

Reaction equation

HRID 356053 reaction equation
[N:1]1[CH:6]=[CH:5][CH:4]=[C:3]([N:7]=[C:8]=[O:9])[CH:2]=1.[Cl:10][C:11]1[CH:12]=[C:13]2[C:17](=[CH:18][C:19]=1[Cl:20])[NH:16][CH2:15][CH2:14]2>>[Cl:10][C:11]1[CH:12]=[C:13]2[C:17](=[CH:18][C:19]=1[Cl:20])[N:16]([C:8](=[O:9])[NH:7][C:3]1[CH:2]=[N:1][CH:6]=[CH:5][CH:4]=1)[CH2:15][CH2:14]2

Participants

3

Reactant 2

HCID 27604933-IsocyanatopyridineHCID 10750101HCID 10750101, compound

Product 1

HCID 10590892HCID 10590892, compound

Procedure

The title compound was prepared as in the method of (Example 2) from 3-pyridylisocyanate and 5,6-dichloroindoline (D39) to give (E20) (1.27 g, 65%) m.p. 236°-238° C.

Workup

  1. customto give (E20) (1.27 g, 65%) m.p. 236°-238° C.

Sources & evidence

ORD record
ord-aae2d970f0194c56bfa5ab9999837ece
Source dataset
uspto-grants-1998_11
Patent number
US05834494

Reaction notes

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