3-Isocyanatopyridine → HCID 10803240, compound

HRID 356055Notes

Reaction equation

HRID 356055 reaction equation
[N:1]1[CH:6]=[CH:5][CH:4]=[C:3]([N:7]=[C:8]=[O:9])[CH:2]=1.[Cl:10][C:11]1[CH:12]=[C:13]2[C:17](=[CH:18][C:19]=1[CH3:20])[NH:16][CH2:15][CH2:14]2>>[Cl:10][C:11]1[CH:12]=[C:13]2[C:17](=[CH:18][C:19]=1[CH3:20])[N:16]([C:8](=[O:9])[NH:7][C:3]1[CH:2]=[N:1][CH:6]=[CH:5][CH:4]=1)[CH2:15][CH2:14]2

Participants

3

Reactant 2

HCID 27604933-IsocyanatopyridineHCID 106546525-Chloro-2,3-dihydro-6-methyl-1H-indole

Product 1

HCID 10803240HCID 10803240, compound

Procedure

The title compound was prepared as in the method of (Example 2) from 3-pyridylisocyanate and 5-chloro-6-methylindoline (D45) to give (E23) (0.76 g, 73%) m.p. 217°-218° C.

Workup

  1. customto give (E23) (0.76 g, 73%) m.p. 217°-218° C.

Sources & evidence

ORD record
ord-b60a843fbe474c538389d59d7f159201
Source dataset
uspto-grants-1998_11
Patent number
US05834494

Reaction notes

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