HCID 18940579, compound → HCID 70112331, compound

HRID 356181Notes

Reaction equation

HRID 356181 reaction equation
[CH:1]1[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH:4]=[CH:3][C:2]=1[CH2:11][N:12]1[C:18](=[O:19])[CH:17]2[CH2:20][CH2:21][CH2:22][C:16]2=[N:15][C:14]2[CH:23]=[CH:24][CH:25]=[CH:26][C:13]1=2>C(OCC)(=O)C.CCCCCC>[CH:1]1[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH:4]=[CH:3][C:2]=1[CH2:11][N:12]1[C:18](=[O:19])[C@H:17]2[CH2:20][CH2:21][CH2:22][C@H:16]2[NH:15][C:14]2[CH:23]=[CH:24][CH:25]=[CH:26][C:13]1=2

Participants

3

Reactant 1

HCID 18940579HCID 18940579, compound

Product 1

HCID 70112331HCID 70112331, compoundYield 81%

Reagents, catalysts & solvents 1

HCID 21226206Ethyl acetate hexaneSolvent

Procedure

Using 9-(2-naphthylmethyl)-2,3,9,10a-tetrahydrobenzo[b]cyclopenta[1,4]diazepin-10(1H)-one, the titled compound was synthesized in substantially the same manner as in yield of 81%, m.p. 148.0°-148.5° C. (ethyl acetate-hexane).

Sources & evidence

ORD record
ord-95c462ed0648444d848add3e5cbb4f7f
Source dataset
uspto-grants-1998_11
Patent number
US05834463

Reaction notes

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