HCID 18940572, compound → HCID 70109358, compound

HRID 356212Notes

Reaction equation

HRID 356212 reaction equation
[CH2:1]([N:8]1[C:14](=[O:15])[CH:13]2[CH2:16][CH2:17][CH2:18][C:12]2=[N:11][C:10]2[CH:19]=[C:20]([N+:23]([O-:25])=[O:24])[CH:21]=[CH:22][C:9]1=2)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1>C(OCC)C>[CH2:1]([N:8]1[C:14](=[O:15])[C@H:13]2[CH2:16][CH2:17][CH2:18][C@H:12]2[NH:11][C:10]2[CH:19]=[C:20]([N+:23]([O-:25])=[O:24])[CH:21]=[CH:22][C:9]1=2)[C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1

Participants

3

Reactant 1

HCID 18940572HCID 18940572, compound

Product 1

HCID 70109358HCID 70109358, compoundYield 89%

Reagents, catalysts & solvents 1

HCID 3283Diethyl EtherSolvent

Procedure

Employing 9-benzyl-6-nitro-2,3,9,10a-tetrahydrobenzo[b]cyclopenta[e][1,4]diazepin-10(1H)-one, the titled compound was synthesized by substantially the same procedure as in Reference Example 15. Yield 89%. m.p.174°-176° C. (diethyl ether).

Sources & evidence

ORD record
ord-c997177a58974895bb634d0b1310daf9
Source dataset
uspto-grants-1998_11
Patent number
US05834463

Reaction notes

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