HCID 18940569, compound → HCID 70110495, compound

HRID 356213Notes

Reaction equation

HRID 356213 reaction equation
[C:1]([C:3]1[CH:24]=[CH:23][C:6]([CH2:7][N:8]2[C:14](=[O:15])[CH:13]3[CH2:16][CH2:17][CH2:18][C:12]3=[N:11][C:10]3[CH:19]=[CH:20][CH:21]=[CH:22][C:9]2=3)=[CH:5][CH:4]=1)#[N:2]>C(OCC)C>[C:1]([C:3]1[CH:4]=[CH:5][C:6]([CH2:7][N:8]2[C:14](=[O:15])[C@H:13]3[CH2:16][CH2:17][CH2:18][C@H:12]3[NH:11][C:10]3[CH:19]=[CH:20][CH:21]=[CH:22][C:9]2=3)=[CH:23][CH:24]=1)#[N:2]

Participants

3

Reactant 1

HCID 18940569HCID 18940569, compound

Product 1

HCID 70110495HCID 70110495, compoundYield 65%

Reagents, catalysts & solvents 1

HCID 3283Diethyl EtherSolvent

Procedure

Employing 9-(4-cyanobenzyl)-2,3,9,10a-tetrahydrobenzo[b]cyclopenta[e][1,4]diazepin-10(1H)-one, the titled compound was synthesized by substantially the same procedure as in Reference Example 15. Yield 65%. m.p.224°-226° C. (decomp.) (diethyl ether).

Sources & evidence

ORD record
ord-0a14dcb296c94ba7874acfabccc92600
Source dataset
uspto-grants-1998_11
Patent number
US05834463

Reaction notes

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