HuagongsheHuagongshe Chemistry Print Report · For research reference only
Imidazole → HCID 18798645, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Imidazole | HCID 795 | — |
| Reactant | tert-Butyldimethylsilyl chloride | HCID 28928 | — |
| Reactant | HCID 12648138 | HCID 12648138 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 18798645 | HCID 18798645 | — |
Reaction Steps
The title compound was prepared as described in General Method 5 using 4.11 g (18.2 mmol) of 3-(3-hydroxy-phenyl)-1-phenyl-propan-1-one from Example M, 1.5 g (22 mmol) of imidazole, 3.0 g (20 mmol) of t-butyldimethylsilyl chloride and 75 mL of CH2Cl2. The product was carried on crude to the next step (see Example UU).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05834506 |
| Source dataset | uspto-grants-1998_11 |
| ORD ID | ord-076a51fb7da94901a793bd5bf6f5f219 |
| Source note | uspto-grants-1998_11 |