HCID 10937203, compound → HCID 15956280, compound

HRID 356597Notes

Reaction equation

HRID 356597 reaction equation
[CH2:1]([N:4]1[C:10]2[N:11]=[CH:12][CH:13]=[CH:14][C:9]=2[C:8](=[O:15])[NH:7][C:6]2[CH:16]=[CH:17][C:18](OS(C(F)(F)F)(=O)=O)=[N:19][C:5]1=2)[CH2:2][CH3:3].C([Sn](CCCC)(CCCC)[C:33]1[CH:34]=[N:35][NH:36][CH:37]=1)CCC>>[CH2:1]([N:4]1[C:10]2[N:11]=[CH:12][CH:13]=[CH:14][C:9]=2[C:8](=[O:15])[NH:7][C:6]2[CH:16]=[CH:17][C:18]([C:33]3[CH:34]=[N:35][NH:36][CH:37]=3)=[N:19][C:5]1=2)[CH2:2][CH3:3]

Participants

3

Reactant 2

HCID 10937203HCID 10937203, compoundHCID 18938881HCID 18938881, compound

Product 1

HCID 15956280HCID 15956280, compound

Procedure

The title compound (mp 291°-292° C.) was prepared from 5,11-dihydro-11-n-propyl-2-trifluoromethanesulfonyloxy-6H-dipyrido[3,2-b:2',3'-e][1,4]diazepin-6-one and 4-(tributylstannyl)pyrazole in a manner analogous to that described in Example 1.

Sources & evidence

ORD record
ord-37b847adfecc4c9bb4b9cf1921a19830
Source dataset
uspto-grants-1998_11
Patent number
US05837704

Reaction notes

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