Nitric Acid → Praseodymium trinitrate

HRID 35666Notes

Reaction equation

HRID 35666 reaction equation
[O-2].[Pr+3:2].[O-2].[O-2].[Pr+3].[N+:6]([O-:9])([OH:8])=[O:7]>>[N+:6]([O-:9])([O-:8])=[O:7].[Pr+3:2].[N+:6]([O-:9])([O-:8])=[O:7].[N+:6]([O-:9])([O-:8])=[O:7]

Participants

3

Reactant 2

HCID 944Nitric AcidHCID 165911Praseodymium oxide

Product 1

HCID 498125Praseodymium trinitrate

Conditions

Temperature
100 °C

Procedure

Praseodymium oxide, Pr6O11 (1.55 g) was weighed into a silica crucible, concentrated nitric acid (2.5 ml) added and heated on a hot plate until the oxide had dissolved and the acid evaporated (~2 hr). The crucible and contents were heated overnight in an oven at 100° C. The praseodymium nitrate was dissolved in water, transferred to a volumetric flask (25 ml) and made up to volume.

Workup

  1. additionadded
  2. dissolutionhad dissolved
  3. customthe acid evaporated (~2 hr)
  4. dissolutionThe praseodymium nitrate was dissolved in water
  5. customtransferred to a volumetric flask

Sources & evidence

ORD record
ord-21f71bdaa0084149be872c2aa3ec65c9
Source dataset
uspto-grants-1988_08
Patent number
US04767792

Reaction notes

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