Aniline → N-(2-methoxyethyl)aniline

HRID 356674Notes

Reaction equation

HRID 356674 reaction equation
[NH2:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[CH3:8][O:9][CH2:10][CH:11]=O>>[CH3:8][O:9][CH2:10][CH2:11][NH:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1

Participants

3

Reactant 2

HCID 6115AnilineHCID 91563Methoxyacetaldehyde

Product 1

HCID 1581105N-(2-methoxyethyl)aniline

Procedure

The title compound was prepared from aniline and methoxyacetaldehyde by the same method as described for Example 5, part A. The residue was purified by flash chromatography on silica gel (ethyl acetate:hexanes/1:15) to give a pale yellow oil.

Workup

  1. customThe residue was purified by flash chromatography on silica gel (ethyl acetate:hexanes/1:15)
  2. customto give a pale yellow oil

Sources & evidence

ORD record
ord-71690d9d8ae248589a78ef48e10e9953
Source dataset
uspto-grants-1998_11
Patent number
US05837702

Reaction notes

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