HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Mercaptophenol → 4-[(4-Hydroxyphenyl)disulfanyl]phenol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Mercaptophenol | HCID 240147 | — |
| Solvent | Dimethyl Sulfoxide | HCID 679 | — |
| Product | 4-[(4-Hydroxyphenyl)disulfanyl]phenol | HCID 280665 | — |
Reaction Steps
p-Hydroxybenzenethiol (25 g) was dissolved in DMSO (155 ml) and the solution was stirred for 4 hours and poured into ice water (1 L). The precipitated crystals were dried under reduced pressure to give bis(p-hydroxyphenyl)disulfide quantitatively.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05840716 |
| Source dataset | uspto-grants-1998_11 |
| ORD ID | ord-7085146c16bc4d318e7e2210028e4e8b |
| Source note | uspto-grants-1998_11 |