HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → 5-(4-Chlorobutylthio)-2-methylimidazo[1,2-a]pyridine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 1-Bromo-4-chlorobutane | HCID 81364 | — |
| Reactant | HCID 178429829 | HCID 178429829 | — |
| Product | 5-(4-Chlorobutylthio)-2-methylimidazo[1,2-a]pyridine | HCID 18936662 | — |
Reaction Steps
Using 657 mg (4.0 mmol) of 5-mercapto-2-methylimidazo-[1,2-a]pyridine, 0.70 ml (5.0 mmol) of triethylamine and 0.58 ml (5.0 mmol) of 1-bromo-4-chlorobutane, the same procedure as in Reference Example 1 was followed, to yield 838 mg (82.3%, light orange solid) of the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05840732 |
| Source dataset | uspto-grants-1998_11 |
| ORD ID | ord-84030f74c3b84c75a4ee38749cf5c5d7 |
| Source note | uspto-grants-1998_11 |