HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → 5-(4-Methanesulfonyloxybutylthio)-imidazo[1,2-c]pyrimidine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Methanesulfonyl chloride | HCID 31297 | — |
| Reactant | 5-(4-Hydroxybutylthio)imidazo[1,2-c]pyrimidine | HCID 18936882 | — |
| Product | 5-(4-Methanesulfonyloxybutylthio)-imidazo[1,2-c]pyrimidine | HCID 18936880 | — |
Reaction Steps
Using 2.23 g (10 mmol) of 5-(4-hydroxybutylthio) imidazo[1,2-c]pyrimidine, 1.53 ml (11 mmol) of triethylamine and 0.85 ml (11 mmol) of methanesulfonyl chloride, the same procedure as in Reference Example 8 was followed, to yield 5-(4-methanesulfonyloxybutylthio)-imidazo[1,2-c]pyrimidine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05840732 |
| Source dataset | uspto-grants-1998_11 |
| ORD ID | ord-9e83855df2c74aa895cd3dcd870a5d9d |
| Source note | uspto-grants-1998_11 |