HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Iodide → 3-[4-(2-Aminopyridin-3-yloxy)butyl]oxazolidine-2,4-dione
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Iodide | HCID 5238 | — |
| Reactant | 2-Amino-3-(4-chlorobutyloxy)pyridine | HCID 18936781 | — |
| Reactant | Oxazolidine-2,4-dione potassium salt | HCID 70204806 | — |
| Product | 3-[4-(2-Aminopyridin-3-yloxy)butyl]oxazolidine-2,4-dione | HCID 18936721 | — |
Reaction Steps
Using 15.05 g (75 mmol) of 2-amino-3-(4-chlorobutyloxy)pyridine, 10.44 g (75 mmol) of oxazolidine-2,4-dione potassium salt and 11.24 g (75 mmol) of sodium iodide, the same procedure as in Reference Example 11 was followed, to yield 12.34 g (62.0%, yellow powder) of the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05840732 |
| Source dataset | uspto-grants-1998_11 |
| ORD ID | ord-4f09fad718ba4004ba974da0e7c46a7d |
| Source note | uspto-grants-1998_11 |