Ammonia → 2-Benzothiazylsulfenamide

HRID 357527Notes

Reaction equation

HRID 357527 reaction equation
[SH:1][C:2]1[S:3][C:4]2[CH:10]=[CH:9][CH:8]=[CH:7][C:5]=2[N:6]=1.[NH3:11].Cl[O-].[Na+]>O>[S:3]1[C:4]2[CH:10]=[CH:9][CH:8]=[CH:7][C:5]=2[N:6]=[C:2]1[S:1][NH2:11]

Participants

5

Reactant 3

HCID 222AmmoniaHCID 23665760Sodium HypochloriteHCID 178418395HCID 178418395, compound

Product 1

HCID 986482-Benzothiazylsulfenamide

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

2-Benzothiazole sulfenamide was synthesized from the reaction of 2-mercaptobenzothiazole, ammonia, and sodium hypochlorite in water (previously incorporated J. Org. Chem., 14, 921 (1940)).

Sources & evidence

ORD record
ord-c81e638ef7f84dd8a969209cd0e2c95d
Source dataset
uspto-grants-1998_11
Patent number
US05840908

Reaction notes

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