HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylamine → 2-[1-(Ethoxyimino)propyl]-3-hydroxy-5-(2,6-dimethyl-3-dimethylsulfamoylphenyl)cyclohex-2-en-1-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylamine | HCID 674 | — |
| Reactant | Chlorosulfonic acid | HCID 24638 | — |
| Reactant | O-ethylhydroxylamine hydrochloride | HCID 76850 | — |
| Reactant | HCID 178458832 | HCID 178458832 | — |
| Product | 2-[1-(Ethoxyimino)propyl]-3-hydroxy-5-(2,6-dimethyl-3-dimethylsulfamoylphenyl)cyclohex-2-en-1-one | HCID 135973980 | — |
Reaction Steps
2-[1-(Ethoxyimino)propyl]-3-hydroxy-5-(2,6-dimethyl-3-dimethylsulfamoylphenyl)cyclohex-2-en-1-one (5) was prepared from 3-hydroxy-5-(2,6-dimethylphenyl)-2-propionylcyclohex-2-en-1-one, chlorosulfonic acid, dimethylamine, and ethoxyamine hydrochloride following essentially the same procedure as that described in Example 5.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04767879 |
| Source dataset | uspto-grants-1988_08 |
| ORD ID | ord-5cb6474f52844c2bba022377de34628a |
| Source note | uspto-grants-1988_08 |