HRID357696

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID284

Formic acid

CH2O2

HCID15346007

1,2,3,4-Tetrafluoro-5-(trichloromethyl)benzene

C7HCl3F4

PRODUCTS

生成物

HCID2733689

2,3,4,5-Tetrafluorobenzoyl chloride

C7HClF4O

收率 93%

AUXILIARIES

试剂、催化剂与溶剂

催化剂HCID24380

未命名化合物

PROCEDURE

实验过程

268 g of 2,3,4,5-tetrafluorobenzotrichloride were added to the distillation residue (approximately 20 g) and 2.7 g of iron(III) chloride were added. The mixture was reacted with formic acid in a similar manner to a). 198 g (93% of theory) of 2,3,4,5-tetrafluorobenzoyl chloride were obtained.

WORKUP

后处理

additionwere added