HCID 18938507, compound → HCID 57309150, compound

HRID 357697Notes

Reaction equation

HRID 357697 reaction equation
[CH2:1]([N:6]([CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH3:25])[C:7](=[O:16])[NH:8][C@H:9]1[CH2:14][CH2:13][CH2:12][CH2:11][C@@H:10]1[OH:15])[C:2]([CH3:5])([CH3:4])C.[CH2:26](NCCCCCCCCC)[C:27](C)(C)[CH3:28].[CH2:41](CCCCCCCCCCN)C1C=CC=CC=1>>[CH2:1]([N:6]([CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH3:41])[C:7](=[O:16])[NH:8][C@H:9]1[CH2:14][CH2:13][CH2:12][CH2:11][C@@H:10]1[OH:15])[C:2]1[CH:4]=[CH:28][CH:27]=[CH:26][CH:5]=1

Participants

4

Reactant 3

HCID 18938507HCID 18938507, compoundHCID 21253339HCID 21253339, compoundHCID 57230105HCID 57230105, compound

Product 1

HCID 57309150HCID 57309150, compoundYield 85%

Procedure

The same procedure for preparing (1S,2S)-2-(3-neopentyl-3-nonylureido)cyclohexanol as in Example 3 was repeated except that the neopentylnonylamine employed in Example 3 was replaced by benzyldecylamine, whereby (1S,2S)-2-(3-benzyl-3-decylureido)cyclohexanol was obtained in a yield of 85%.

Sources & evidence

ORD record
ord-6ff4429fb9d443f7bdccac137c1f385c
Source dataset
uspto-grants-1998_11
Patent number
US05840977

Reaction notes

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