N-(1-Methylethyl)-1-decanamine → HCID 57094078, compound

HRID 357698Notes

Reaction equation

HRID 357698 reaction equation
C(N(CCCCCCCCC)[C:7](=[O:16])[NH:8][C@H:9]1[CH2:14][CH2:13][CH2:12][CH2:11][C@@H:10]1[OH:15])C(C)(C)C.C(NCCCCCCCCC)C(C)(C)C.[CH2:41]([NH:51][CH:52]([CH3:54])[CH3:53])[CH2:42][CH2:43][CH2:44][CH2:45][CH2:46][CH2:47][CH2:48][CH2:49][CH3:50]>>[CH2:41]([N:51]([CH:52]([CH3:53])[CH3:54])[C:7](=[O:16])[NH:8][C@H:9]1[CH2:14][CH2:13][CH2:12][CH2:11][C@@H:10]1[OH:15])[CH2:42][CH2:43][CH2:44][CH2:45][CH2:46][CH2:47][CH2:48][CH2:49][CH3:50]

Participants

4

Reactant 3

HCID 12738007N-(1-Methylethyl)-1-decanamineHCID 18938507HCID 18938507, compoundHCID 57230105HCID 57230105, compound

Product 1

HCID 57094078HCID 57094078, compoundYield 88%

Procedure

The same procedure for preparing (1S,2S)-2-(3-neopentyl-3-nonylureido)cyclohexanol as in Example 3 was repeated except that the neopentylnonylamine employed in Example 3 was replaced by decylisopropylamine, whereby (1S,2S)-2-(3-decyl-3-isopropylureido)cyclohexanol was obtained in a yield of 88%.

Sources & evidence

ORD record
ord-25fe3a4c1269444d8848add9b0b54682
Source dataset
uspto-grants-1998_11
Patent number
US05840977

Reaction notes

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