HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzene, (2-bromoethoxy)- → HCID 53846490, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzene, (2-bromoethoxy)- | HCID 68526 | — |
| Reactant | Benzenesulfonothioic acid, 4-methyl-, potassium salt (1:1) | HCID 23662126 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 53846490 | HCID 53846490 | — |
Reaction Steps
The title compound was prepared as described in General Method 2 using 2-phenoxyethyl bromide (0.025 mmol), potassium thiotosylate (0.025 mmol) and DMF (100 mL) to give a solid. 1H NMR (CDCl3) δ 2.45 (s, 3 H), 3.34 (t, 2 H), 4.14 (t, 2 H), 6.80 (d, 2 H), 6.95 (t, 1 H), 7.26 (t, 2 H), 7.35 (d, 2 H), 7.82 (d, 2 H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05840751 |
| Source dataset | uspto-grants-1998_11 |
| ORD ID | ord-88220c8332a4487fbd6b363d2ee99353 |
| Source note | uspto-grants-1998_11 |