HuagongsheHuagongshe Chemistry Print Report · For research reference only
Propanal → HCID 56622747, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Propanal | HCID 527 | — |
| Reactant | HCID 20450261 | HCID 20450261 | — |
| Reactant | HCID 56638720 | HCID 56638720 | — |
| Product | HCID 56622747 | HCID 56622747 | 80% |
Reaction Steps
A mixture of Δ3 -4-tert.-butyl- and Δ3 -3-tert.-butyl-tetrahydrobenzaldehyde prepared according to instructions B is condensed with propionaldehyde in a conventional manner. An 80% yield of 2-methyl-(4-tert.-butyl-cyclohex-3-enyl)-prop-2-en-1-al and 2-methyl-(3-tert.-butyl-cyclohex-3-enyl)-prop-2-en-1-al in a ratio of about 70:30 is obtained. Boiling point: 153° C./30 mbar.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04464370 |
| Source dataset | uspto-grants-1984_08 |
| ORD ID | ord-40ddd4f99abf4b69a1ba6b69e0175c80 |
| Source note | uspto-grants-1984_08 |