HRID358233

反应详情

EQUATION

反应方程式

HRID 358233 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

The mixture which was homogenised consisted of 119 g of titanium trichloride, 26 cm3 of butyl benzoate, 390 cm3 of toluene and 3 g of polystyrene ("Lustrex" HF 66). After operating the homogeniser at maximum power for 2.75 minutes, the contents of the flask had formed an immobile gel-like product and the temperature had risen to above 50° C. Homogenisation was terminated and 500 cm3 of toluene were added to assist in the transfer of the dispersed solid to a storage vessel.

WORKUP

后处理

  1. customfor 2.75 minutes
  2. customthe contents of the flask had formed an immobile gel-like product
  3. customhad risen to above 50° C
  4. customHomogenisation was terminated
  5. addition500 cm3 of toluene were added
  6. customto assist in the transfer of the dispersed solid to a storage vessel