HRID358233
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
The mixture which was homogenised consisted of 119 g of titanium trichloride, 26 cm3 of butyl benzoate, 390 cm3 of toluene and 3 g of polystyrene ("Lustrex" HF 66). After operating the homogeniser at maximum power for 2.75 minutes, the contents of the flask had formed an immobile gel-like product and the temperature had risen to above 50° C. Homogenisation was terminated and 500 cm3 of toluene were added to assist in the transfer of the dispersed solid to a storage vessel.
WORKUP
后处理
- customfor 2.75 minutes
- customthe contents of the flask had formed an immobile gel-like product
- customhad risen to above 50° C
- customHomogenisation was terminated
- addition500 cm3 of toluene were added
- customto assist in the transfer of the dispersed solid to a storage vessel