HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 53749658, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | 2-Methylpyridine | HCID 7975 | — |
| Reactant | Ammonium nitrate | HCID 22985 | — |
| Reactant | Ethyl orthoformate | HCID 31214 | — |
| Reactant | HCID 56988318 | HCID 56988318 | — |
| Product | HCID 53749658 | HCID 53749658 | — |
Reaction Steps
100 g of 2,5-diformyl-2,4-hexadiene, 1 g of ammonium nitrate, 192 g of triethoxymethane and 200 ml of dry ethanol are stirred at 20° for 48 hours; the mixture is neutralized with α-picoline; the solvent is distilled off; and, after purifying the residue by distillation, 1,1,6,6-tetraethoxy-2,5-dimethyl-2,4-hexadiene is obtained, b.p.=135°-139°/0.2 mm Hg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04466805 |
| Source dataset | uspto-grants-1984_08 |
| ORD ID | ord-e83f43e003a2422989d5737f390c9503 |
| Source note | uspto-grants-1984_08 |