Water → 3,3,6,6-Tetramethylpiperazin-2-one

HRID 358324Notes

Reaction equation

HRID 358324 reaction equation
[CH3:1][C:2]([CH3:6])(O)[C:3]#[N:4].[OH2:7]>>[CH3:1][C:2]1([CH3:6])[NH:4][CH2:3][C:2]([CH3:6])([CH3:1])[NH:4][C:3]1=[O:7]

Participants

3

Reactant 2

HCID 962WaterHCID 6406Acetone Cyanohydrin

Product 1

HCID 199139303,3,6,6-Tetramethylpiperazin-2-one

Procedure

In a manner analogous to that described in example 3A above, 2,methyl-1,2-diaminopropane, water and acetone cyanohydrin are reacted, and the reaction product recovered. When dissolved in acetone and recrystallized it is identified as 3,3,6,6-tetramethyl-2-piperazinone.

Workup

  1. customthe reaction product recovered
  2. dissolutionWhen dissolved in acetone
  3. customrecrystallized it

Sources & evidence

ORD record
ord-c4d66142736b46fd9fc640446510a548
Source dataset
uspto-grants-1984_08
Patent number
US04466916

Reaction notes

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