HRID358387

反应详情

EQUATION

反应方程式

HRID 358387 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

t-Butyl hypochlorite (22.8 g, 0.21 mole) was added to 1,1-di(p-fluorophenyl)urea (49.4 g, 0.2 mole) in 750 ml methanol at 0°-5° and the mixture stirred for 0.5 hour to produce a thin slurry containing step (a) title product.

WORKUP

后处理

  1. customto produce a thin slurry