HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 20264132, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 12873134 | HCID 12873134 | — |
| Catalyst | Dimethylformamide | HCID 6228 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 20264132 | HCID 20264132 | — |
Reaction Steps
A mixture of 6,7-diacetoxy-1-ethyl-1,4-dihydro-4-oxoquinoline-3-caroxylic acid (60 mg), thionyl chloride (40 μL), and dimethylformamide (one drop) was heated under reflux for 3 hours in benzene (40 mL), and then the solvent was evaporated. To the residue was added benzene (20 mL). Benzene was evaporated and the residue was vacuum dried to give 6,7-diacetoxy-1-ethyl-1,4-dihydro-4-oxoquinoline-3-carbonyl chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04468394 |
| Source dataset | uspto-grants-1984_08 |
| ORD ID | ord-6d4f069b2b0142928320fcdb33bf7e8a |
| Source note | uspto-grants-1984_08 |