HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzene → HCID 15582461, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzene | HCID 241 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 15582460 | HCID 15582460 | — |
| Catalyst | Dimethylformamide | HCID 6228 | — |
| Solvent | Hexane | HCID 8058 | — |
| Product | HCID 15582461 | HCID 15582461 | — |
Reaction Steps
A mixture of 6,7-diacetoxy-2-oxo-2H-1-benzopyran-3-carboxylic acid (306 mg), thionyl chloride (80 μL), dimethyl formamide (one drop), and benzene (15 mL) was refluxed for 1 hour. After cooling to room temperature, hexane (10 mL) was added. Solids were filtered off to give 6,7-diacetoxy-2-oxo-2H-1-benzopyran-3-carbonyl chloride (286 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04468394 |
| Source dataset | uspto-grants-1984_08 |
| ORD ID | ord-a7024a0f719a4a1ea9933cfe4a6ec0cd |
| Source note | uspto-grants-1984_08 |