HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 13369869, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Benzoyl chloride, 3-chloro- | HCID 69252 | — |
| Reactant | HCID 13369865 | HCID 13369865 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 13369869 | HCID 13369869 | — |
Reaction Steps
1.0 Gram of 6-(1-piperazinylcarbonyl)carbostyril monohydrochloride, 0.72 g of m-chlorobenzoylchloride and 1.4 ml of triethylamine were suspended in 15 ml of dichloromethane and the suspension was stirred at a room temperature for 2 hours. Crystals formed in the reaction mixture were collected by filtration and recrystallized from dimethylformamide to obtain 1.07 g of 6-[4-(3-chlorobenzoyl)-1-piperazinylcarbonyl]-carbostyril. Colorless powdery crystals. Melting point: over 300° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04468402 |
| Source dataset | uspto-grants-1984_08 |
| ORD ID | ord-b1c86db619cb4c6494beccc883d0e8e7 |
| Source note | uspto-grants-1984_08 |