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HRID 358540作成日:2026年10月25日

Ethyl 4,6,6-trichloro-3,3-dimethyl-5-hexenoate → 2(3H)-Furanone, 5-(2,2-dichloroethenyl)dihydro-4,4-dimethyl-

https://huagongshe.com/reaction/358540

反応式

関与物質

役割名称HCID仕込み量
反応物Ethyl 4,6,6-trichloro-3,3-dimethyl-5-hexenoateHCID 3042523—
反応物5-Hexenoic acid, 4,6,6-trichloro-3,3-dimethyl-, methyl esterHCID 10999791—
生成物2(3H)-Furanone, 5-(2,2-dichloroethenyl)dihydro-4,4-dimethyl-HCID 1019820395%

反応手順

The above procedure was repeated except that 27.4 parts of ethyl 3,3-dimethyl-4,6,6-trichloro-5-hexenoate was used in lieu of methyl 3,3-dimethyl-4,6,6-trichloro-5-hexenoate. In this case, 19.8 parts of 3,3-dimethyl-4-(2',2'-dichlorovinyl)-4-butanolide was obtained (yield 95%).

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US04468521
出典データセットuspto-grants-1984_08
ORD IDord-af22ec5b42ba4adeb1f9266970015679
出典メモuspto-grants-1984_08