Potassium Carbonate → HCID 20066943, compound

Participants

Reaction Steps

A mixture of 4-chlorobenzenesulphonamide (4.5 g), ethyl 8-bromo-2,2-dimethyloctanoate (3.3 g) and potassium carbonate (9.3 g) in dry methylethylketone (140 ml) was refluxed for 9 hours. The inorganic residues were removed by filtration and the filtrate was evaporated to dryness to give an oil. Chromatography on silica gel eluted with chloroform-petroleum ether 15:1 gave the title compound (1.05 g) as an oil.

Provenance & Evidence