Benzenesulfonyl chloride → HCID 20066939, compound

Participants

Reaction Steps

A solution of 9-aminononanenitrile (2.0 g) in pyridine (60 ml) was treated with benzenesulphonyl chloride (2.29 g) in pyridine (10 ml). The solution was stirred for 18 hours when the solvent was removed in vacuo. The residue was dissolved in dilute hydrochloric acid and extracted with chloroform. The chloroform extract was dried over magnesium sulphate, the solvent was removed and the residue was chromatographed on silica gel eluted with chloroform to give the title compound (0.74 g) as a low melting solid.

Provenance & Evidence