Sodium Hydroxide → HCID 20066985, compound
Reaction equation
C([O:3][C:4](=[O:27])[C:5]([CH3:26])([CH3:25])[CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][NH:14][S:15]([C:18]1[CH:23]=[CH:22][C:21]([Cl:24])=[CH:20][CH:19]=1)(=[O:17])=[O:16])C.[OH-].[Na+]>>[CH3:25][C:5]([CH3:26])([CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][NH:14][S:15]([C:18]1[CH:23]=[CH:22][C:21]([Cl:24])=[CH:20][CH:19]=1)(=[O:16])=[O:17])[C:4]([OH:27])=[O:3]Participants
3
Procedure
Ethyl-10-(4-chlorobenzenesulphonamido)-2,2-dimethyldecanoate (1.4 g, 0.003 mol) was treated with sodium hydroxide by the method described in Example 5(iii) to give the title compound which was recrystallised from ether/pet. ether (0.59 g, m.p. 78°-9° C.).
Sources & evidence
- ORD record
- ord-20a0a368a35f42a39a87180b09b0b996
- Source dataset
- uspto-grants-1991_03
- Patent number
- US04997847
Reaction notes
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