HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chlorobenzenesulfonyl chloride → 7-(4-Chlorobenzenesulphonamido)heptanoic Acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chlorobenzenesulfonyl chloride | HCID 7398 | — |
| Reactant | 7-Aminoheptanoic acid | HCID 13580 | — |
| Solvent | Sodium Hydroxide | HCID 14798 | — |
| Product | 7-(4-Chlorobenzenesulphonamido)heptanoic Acid | HCID 20066980 | — |
Reaction Steps
A solution of 7-aminoheptanoic acid in 10% sodium hydroxide solution was treated with 4-chlorobenzenesulphonyl chloride in the manner of Example 1 to give the title compound which, after recrystallisation from aqueous ethanol, had a melting point of 128°-129° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04997847 |
| Source dataset | uspto-grants-1991_03 |
| ORD ID | ord-c812be37b9ed44eb8f0793de2ca21202 |
| Source note | uspto-grants-1991_03 |