Benzenesulfonyl chloride, 3,4-dichloro- → HCID 20066963, compound

HRID 358635Notes

Reaction equation

HRID 358635 reaction equation
[NH2:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][C:9]([OH:11])=[O:10].[Cl:12][C:13]1[CH:14]=[C:15]([S:20](Cl)(=[O:22])=[O:21])[CH:16]=[CH:17][C:18]=1[Cl:19]>>[Cl:12][C:13]1[CH:14]=[C:15]([S:20]([NH:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][C:9]([OH:11])=[O:10])(=[O:21])=[O:22])[CH:16]=[CH:17][C:18]=1[Cl:19]

Participants

3

Reactant 2

HCID 7383Benzenesulfonyl chloride, 3,4-dichloro-HCID 660858-Aminooctanoic acid

Product 1

HCID 20066963HCID 20066963, compound

Procedure

8-Aminooctanoic acid (1.0 g, 0.006 mol) was treated with 3,4-dichlorobenzenesulphonylchloride (1.54 g, 0.006 mol), according to the method described in Example 4, to give the title compound which was recrystallised from 2-propanol/water (1.2 g, m.p. 115°-6° C.).

Sources & evidence

ORD record
ord-ebb31a7e19a142ff89240131d8ada64b
Source dataset
uspto-grants-1991_03
Patent number
US04997847

Reaction notes

Loading…