6-Aminohexanoic Acid → HCID 1965826, compound

HRID 358637Notes

Reaction equation

HRID 358637 reaction equation
[NH2:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][C:7]([OH:9])=[O:8].[Cl:10][C:11]1[CH:16]=[CH:15][C:14]([S:17](Cl)(=[O:19])=[O:18])=[CH:13][CH:12]=1>>[Cl:10][C:11]1[CH:16]=[CH:15][C:14]([S:17]([NH:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][C:7]([OH:9])=[O:8])(=[O:19])=[O:18])=[CH:13][CH:12]=1

Participants

3

Reactant 2

HCID 5646-Aminohexanoic AcidHCID 73984-Chlorobenzenesulfonyl chloride

Product 1

HCID 1965826HCID 1965826, compound

Procedure

6-Aminohexanoic acid (2.62 g, 0.02 mol) was treated with 4-chlorobenzenesulphonyl chloride (4.22 g, 0.02 mol) by the method described in Example 4 to give the title compound which was recrystallised from ethylacetate-ether (1.92 g, m.p. 126°-7° C.

Sources & evidence

ORD record
ord-5c3cdd1d88f04dcf884cc5116916cf34
Source dataset
uspto-grants-1991_03
Patent number
US04997847

Reaction notes

Loading…