HuagongsheHuagongshe Chemistry Print Report · For research reference only
8-Aminooctanoic acid → 8-(2,5-Dichloro-3-thienylsulphonamido)octanoic Acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 8-Aminooctanoic acid | HCID 66085 | — |
| Reactant | 2,5-Dichlorothiophene-3-sulfonyl chloride | HCID 2736094 | — |
| Product | 8-(2,5-Dichloro-3-thienylsulphonamido)octanoic Acid | HCID 20066982 | — |
Reaction Steps
8-Aminocaprylic acid (1.0 g, 0.006 mole) was treated with 2,5-dichloro-3-thiophene sulphonyl chloride (1.58 g, 0.006 mole) according to the method described in Example 4 to give the title compound after recrystallisation from isopropanol/water (1.1 g, m.p. 92°-93° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04997847 |
| Source dataset | uspto-grants-1991_03 |
| ORD ID | ord-45be2263488a46599ac7cf730344e2d1 |
| Source note | uspto-grants-1991_03 |