HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Dodecanethiol → HCID 20067258, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Dodecanethiol | HCID 8195 | — |
| Reactant | 10-Bromo-1,8-dihydroxy-10H-anthracen-9-one | HCID 276504 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 20067258 | HCID 20067258 | 85% |
Reaction Steps
10-Bromo-1,8-dihydroxy-9-anthrone (75 mg) was dissolved in dichloromethane (5 ml) and 1-dodecanethiol (0.06 ml) was added. The solution was stirred at room temperature for 7 hours. Removal of the solvent gave a yellow solid which was then recrystallised from absolute ethanol to give 1,8-dihydroxy-10-dodecylthio-9-anthrone (89 mg, 85%) as pale yellow needles, melting point 76° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04997961 |
| Source dataset | uspto-grants-1991_03 |
| ORD ID | ord-35c4940c5bc641188a253e15aed497e6 |
| Source note | uspto-grants-1991_03 |