HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,6-Dibromohexane → 1-[2-[(6-Bromohexyl)oxy]ethyl]naphthalene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,6-Dibromohexane | HCID 12368 | — |
| Reactant | Naphthalen-1-ethanol | HCID 13047 | — |
| Product | 1-[2-[(6-Bromohexyl)oxy]ethyl]naphthalene | HCID 19101837 | 74% |
Reaction Steps
1-Naphthaleneethanol (3.00 g) and 1,6-dibromohexane (12.73 g) were treated according to the method of Intermediate 1. FCC eluting with cyclohexane followed by ethyl acetate-cyclohexane (1:20, then 1:4) gave the title compound (4.32 g) as a colourless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04997986 |
| Source dataset | uspto-grants-1991_03 |
| ORD ID | ord-e2883fd4c9084e1baf143fc31f88a3df |
| Source note | uspto-grants-1991_03 |