HRID358917

反应详情

EQUATION

反应方程式

HRID 358917 的结构方程式

PROCEDURE

实验过程

1-Naphthalenemethanol (6.00 g) and 1,5-dibromopentane (11.5 ml) were treated according to the method of Intermediate 1. FCC eluting with ether-cyclohexane (1:49→2:48) gave the title compound as a colourless oil (8.41 g), t.l.c. (Cyclohexane-ether 19:1) Rf 0.22;

WORKUP

后处理

  1. washFCC eluting with ether-cyclohexane (1:49→2:48)