HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-tert-butyl-N-ethoxalyl-o-phenylenediamine → 1-Tert-butyl-1,2,3,4-tetrahydro-2,3-dioxoquinoxaline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-tert-butyl-N-ethoxalyl-o-phenylenediamine | HCID 67794531 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | 1-Tert-butyl-1,2,3,4-tetrahydro-2,3-dioxoquinoxaline | HCID 10608855 | — |
Reaction Steps
The neat crystals of N-tert-butyl-N-ethoxalyl-o-phenylene diamine (88 g) were heated to 100° C. for 4 h. The crude product hereby deposited from the melt as crystals. After cooling to ambient temperature the solid taken in ether and the product was filtered off as white crystals, m.p. >300° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04999353 |
| Source dataset | uspto-grants-1991_03 |
| ORD ID | ord-0361206192cb4eeea5b97e2deaa46f71 |
| Source note | uspto-grants-1991_03 |