HCID 10490151, compound → HCID 178456567, compound

HRID 358960Notes

Reaction equation

HRID 358960 reaction equation
ClC1C=CC=C2C=1N(C(C)C)C(=O)C(=O)N2.Cl[C:18]1[CH:34]=[CH:33][CH:32]=[C:31]([N+:35]([O-:37])=O)[C:19]=1[N:20]([C:24]([C:26](OCC)=[O:27])=[O:25])[CH:21]([CH3:23])[CH3:22]>C(Cl)Cl>[CH:21]([N:20]1[C:19]2[C:31](=[CH:32][CH:33]=[CH:34][CH:18]=2)[N+:35]([O-:37])=[C:26]([OH:27])[C:24]1=[O:25])([CH3:23])[CH3:22]

Participants

4

Reactant 2

HCID 10490151HCID 10490151, compoundHCID 20065640HCID 20065640, compound

Product 1

HCID 178456567HCID 178456567, compound

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent

Procedure

In a similar manner 8-chloro-1,2,3,4-tetrahydro-1-isopropyl-2,3-dioxo-quinoxaline was prepared from 2-chloro-N-ethoxalyl-N-isopropyl-6-nitroaniline by hydrogenation using methylene chloride as solvent. M.p. 228°-229° C.

Sources & evidence

ORD record
ord-81c5c82c566f4127b0bcf58da6c9375c
Source dataset
uspto-grants-1991_03
Patent number
US04999354

Reaction notes

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