HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → Brl 52974
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 2-(3,4-Dichlorophenyl)acetyl chloride | HCID 2758149 | — |
| Reactant | 4-(Pyrrolidin-1-yl)methyl-4,5,6,7-tetrahydroimidazo[4,5-c]pyridine | HCID 20065697 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | Brl 52974 | HCID 10000638 | — |
Reaction Steps
Prepared as Example No. 12, from 900 mg (4.37 mmoles) of 4-(pyrrolidin-1-yl)methyl-4,5,6,7-tetrahydroimidazo[4,5-c]pyridine, 950 mg (6.88 mmoles) of anhydrous potassium carbonate and 1.30 g (5.80 mmoles) of 3,4-dichlorophenylacetyl chloride in 35 ml of dry chloroform.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04999359 |
| Source dataset | uspto-grants-1991_03 |
| ORD ID | ord-d1934ed4ebf3427e8197c3d0825c7e9b |
| Source note | uspto-grants-1991_03 |