2,6-Xylyl isocyanate → HCID 14555251, compound

HRID 359040Notes

Reaction equation

HRID 359040 reaction equation
[CH3:1][C:2]1[CH:7]=[CH:6][CH:5]=[C:4]([CH3:8])[C:3]=1[N:9]=[C:10]=[O:11].[CH3:12][C:13]1([CH3:26])[C:22]2[C:17](=[CH:18][CH:19]=[CH:20][CH:21]=2)[C:16]([CH3:24])([CH3:23])[CH2:15][CH:14]1[NH2:25]>>[CH3:8][C:4]1[CH:5]=[CH:6][CH:7]=[C:2]([CH3:1])[C:3]=1[NH:9][C:10]([NH:25][CH:14]1[CH2:15][C:16]([CH3:24])([CH3:23])[C:17]2[C:22](=[CH:21][CH:20]=[CH:19][CH:18]=2)[C:13]1([CH3:26])[CH3:12])=[O:11]

Participants

3

Reactant 2

HCID 987872,6-Xylyl isocyanateHCID 15124030HCID 15124030, compound

Product 1

HCID 14555251HCID 14555251, compound

Procedure

Using the method of Example 1, but starting with 2,6-dimethylphenyl isocyanate and 1,2,3,4-tetrahydro-1,1,4,4-tetramethyl-2-naphthylamine, there was obtained N-(2,6-dimethylphenyl)-N'-(1,2,3,4-tetrahydro-1,1,4,4-tetramethyl-2-naphthalenyl)urea, mp 216°-218° C.

Sources & evidence

ORD record
ord-c07c444b4486453f883fcbb3533a6d4d
Source dataset
uspto-grants-1991_03
Patent number
US04999373

Reaction notes

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