HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,1-Dimethylhydrazine → HCID 54468337, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,1-Dimethylhydrazine | HCID 5976 | — |
| Reactant | 2-Propenal, 2-methoxy- | HCID 11389356 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 54468337 | HCID 54468337 | 66.1% |
Reaction Steps
6.4 g of 2-methoxyacrolein are stirred for 1 hour at 30°-35° C. with 4.4 g of N,N-dimethylhydrazine in 50 ml of ether, dried at 20° C. with Na2SO4 and then the solvent is removed. Distillation at 74°-76° C./13 mbar gives 6.2 g of pure 2-methoxy-4-dimethylamino-4-azabutadiene.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04999426 |
| Source dataset | uspto-grants-1991_03 |
| ORD ID | ord-3e8bd73790e24c7db9db22dd813cbd3e |
| Source note | uspto-grants-1991_03 |