HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Methyl-2-buten-1-OL → Ethyl 3,3-dimethylpent-4-enoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Methyl-2-buten-1-OL | HCID 11173 | — |
| Reactant | Ethyl ortho-acetate | HCID 86598186 | — |
| Catalyst | Phosphoric Acid | HCID 1004 | — |
| Product | Ethyl 3,3-dimethylpent-4-enoate | HCID 82262 | 79% |
Reaction Steps
A mixture of 4.3 g of 3-methyl-2-buten-1-ol, 16.2 g of ethyl orthoacetate and 3 drops of phosphoric acid was reacted as described in Example V A to give 6.15 g (79% yield) of ethyl 3,3-dimethyl-4-pentenoate, b.p. 87°-88°/58 mm.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04999451 |
| Source dataset | uspto-grants-1991_03 |
| ORD ID | ord-3e7cb3b1ca404cda836c93bd7abb5b97 |
| Source note | uspto-grants-1991_03 |