HCID 12274415, compound → HCID 15077157, compound

HRID 359220Notes

Reaction equation

HRID 359220 reaction equation
[O:1]1[C:5]([C:6](OCC)=[O:7])=[CH:4][C:3]2[CH:11]=[CH:12][C:13]3[CH:14]=[CH:15][C:16]4[CH:17]=[CH:18][CH:19]=[CH:20][C:21]=4[C:22]=3[C:2]1=2>C(Cl)Cl.CCCCCC>[O:1]1[C:5]([CH2:6][OH:7])=[CH:4][C:3]2[CH:11]=[CH:12][C:13]3[CH:14]=[CH:15][C:16]4[CH:17]=[CH:18][CH:19]=[CH:20][C:21]=4[C:22]=3[C:2]1=2

Participants

3

Reactant 1

HCID 12274415HCID 12274415, compound

Product 1

HCID 15077157HCID 15077157, compoundYield 91%

Reagents, catalysts & solvents 1

HCID 21226440Methylenechloride HexaneSolvent

Procedure

Using the procedure outlined in Example 14A, ethyl phenanthro[4,3-b]furan-2-carboxylate (H. G. Pars Pharmaceutical Laboratories, Inc.) gave a 91% yield of phenanthro[4,3-b]furan-2-methanol, mp 125°-126°, (C,H), (CH2Cl2 /hexane).

Sources & evidence

ORD record
ord-57c3562882584754b8d2bcf5054f5679
Source dataset
uspto-grants-1991_03
Patent number
US04999369

Reaction notes

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